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- W1998975148 abstract "Kinetics of holocellulose hydrolysis in concentrated sulfuric acid was analyzed using <TEX>$^1H$</TEX>-NMR spectroscopy with different reaction time, temperature and acid concentration in secondary hydrolysis. In this work, reaction condition of secondary hydrolysis was similar to concentrated sulfuric acid process with electrodialysis or simulated moving bed chromatography process for sulfuric acid recycling. By <TEX>$^1H$</TEX>-NMR spectroscopy, acid hydrolyzates from higher secondary acid hydrolysis (25-35% acid concentration) was successfully analyzed without any difficulties in neutralization or adsorption of acid hydrolyzate to solid salt. Higher acid concentration, higher temperature and longer reaction time led to more cellulose for glucose conversion but accompanied with glucose to galactose isomerization, glucose to unknown compounds and degradation of glucose to organic acid via furans." @default.
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- W1998975148 date "2014-06-01" @default.
- W1998975148 modified "2023-10-14" @default.
- W1998975148 title "Analysis of secondary reactions in concentrated sulfuric acid hydrolysis of hollocellulose by 1H-NMR spectroscopy" @default.
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- W1998975148 doi "https://doi.org/10.7584/ktappi.2014.46.3.037" @default.
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