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- W1998987150 abstract "Spinosad is a naturally derived insect-control agent for use on cotton and a variety of other crops. A method is described for the determination of spinosad and its major metabolites in beef and poultry meat, milk, cream, and eggs. The method determines residues of the active ingredients (spinosyns A and D) and two metabolites (spinosyn B and N-demethylspinosyn D). For chicken fat, the method has a limit of quantitation (LOQ) of 0.02 μg/g and a limit of detection (LOD) of 0.006 μg/g. For all other chicken tissues, beef tissues, milk, cream, and eggs, the method has an LOQ of 0.01 μg/g and an LOD of 0.003 μg/g. The analytes are extracted from the various sample types using appropriate solvents, and the extracts are purified by liquid−liquid partitioning and solid-phase extraction. All four analytes are determined simultaneously in the purified extracts by reversed-phase high-performance liquid chromatography with ultraviolet detection at 250 nm. Keywords: Spinosad; spinosyn A; spinosyn D; spinosyn B; N-demethylspinosyn D; beef; poultry; chicken; meat; milk, cream; eggs; quantitation; HPLC-UV" @default.
- W1998987150 created "2016-06-24" @default.
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- W1998987150 date "1998-10-24" @default.
- W1998987150 modified "2023-10-01" @default.
- W1998987150 title "Determination of Spinosad and Its Metabolites in Meat, Milk, Cream, and Eggs by High-Performance Liquid Chromatography with Ultraviolet Detection" @default.
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- W1998987150 doi "https://doi.org/10.1021/jf9802326" @default.
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