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• W1999282060 abstract "Starting from tetrakis(trimethylsilyl)stannane, the tris(trimethylsilyl)stannyl alkali derivatives (Me3Si)3SnM, (M = Li, Na, K, Rb, Cs) were prepared in excellent yields. Reaction with MgBr2 · Et2O afforded bis[tris(trimethylsilyl)stannyl]magnesium. Reaction products were investigated by means of multinuclear NMR spectroscopy. At low temperatures, coupling of 7Li and 119Sn between [(Me3Si)3Sn]− and [Li · 3THF]+ (337 Hz) or [Li · 12Cr4]+ (275 Hz), was observed. NMR chemical shifts and coupling constants of the stannyl anions exhibit a strong dependency on the nature of the cation, solvent system, concentration and temperature. In addition, the molecular structure of tris(trimethylsilyl)stannyl sodium · 15Cr5 was determined by X-ray crystallography. The [Na · 15Cr5]+ and [(Me3Si)3Sn]− units are joined by a direct Sn–Na contact, 3.0775(18) Å in length." @default.
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• W1999282060 date "2005-07-01" @default.
• W1999282060 modified "2023-09-26" @default.
• W1999282060 title "Tris(trimethylsilyl)stannyl alkali derivatives: Syntheses and NMR spectroscopic properties" @default.
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• W1999282060 doi "https://doi.org/10.1016/j.ica.2005.04.006" @default.
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