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- W1999407022 abstract "Abstract A reaction between 6-methylfulvene and lithium diisopropylamide in THF solution produces vinylcyclopentadienyllithium in yields of 85–95%. The 1H NMR spectrum of this air-sensitive organlithium reagent has been recorded in THF-d8. Reactions of vinylcyclopentadienyllithium with Group VIB metal hexacarbonyls followed by treatment with N-methyl-N-nitroso-p-toluenesulfonamide afford the new vinyl organometallic monomers (η5-C5H4CHCH2)M(CO)2(NO) (M = Mo, W). Vinylcyclopentadienyllithium also serves as a convenient precursor to a series of (η5-vinylcyclopentadienyl)dicarbonylmetal monomers of cobalt, rhodium, and iridium. The 1H NMR spectra of these vinylcyclopentadienylmetal derivatives have been compared as a function of the metal." @default.
- W1999407022 created "2016-06-24" @default.
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- W1999407022 date "1983-07-01" @default.
- W1999407022 modified "2023-09-23" @default.
- W1999407022 title "The synthesis and 1H NMR study of vinyl organometallic monomers: (η5-C5H4CHCH2)M(CO)2(NO) (M = Cr, Mo, W) and (η5-C5H4CHCH2)M(CO)2 (M = Co, Rh, Ir)" @default.
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- W1999407022 doi "https://doi.org/10.1016/0022-328x(83)85060-8" @default.
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