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- W1999461935 abstract "Infrared spectroscopic studies have shown that transannular interactions occur in 4-t-butyl-3,3,6,6-tetramethyl-1-thiacycloheptan-4-ol (VI). These interactions do not occur in 3,3,6,6-tetramethyl-1-thiacycloheptan-4-ol (III) and only to a minor extend in 3,3,4,6,6-pentamethyl-1-thiacycloheptan-4-ol (IV) and in 3,3,6,6-tetramethyl-4-isopropyl-1-thiacycloheptan-4-ol (V). Treatment of 3,3,6,6-tetramethyl-1-thiacycloheptane-4,5-diol (XVI) with acid gave a transannular rearrangement involving participation of the sulfur atom to 3,3,6,6-tetramethyl-1-oxa-4-thiabicyclo[3.3.0]octane (XVII). Treatment of 5-hydroxy-3,3,6,6-tetramethyl-1-thiacycloheptan-4-one with triphenyl-phosphine dibromide gave a transannular rearrangement to 2-isobutylidene-4,4-dimethyl-3-oxotetrahydrothiophene (XXVII)." @default.
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- W1999461935 date "2010-09-02" @default.
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- W1999461935 title "Transannular interactions and reactions in a seven-membered heterocyclic ring-system" @default.
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- W1999461935 doi "https://doi.org/10.1002/recl.19690880813" @default.
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