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- W1999462910 abstract "Nanocrystalline Al2O3–ZrO2 powder was synthesized by a simple method using oxalic acid as a chelating agent. The formation temperature of α - Al2O3 was investigated by differential thermal analysis. X-ray diffraction (XRD) analysis shows that t-ZrO2 was stabilized in alumina matrix with oxalic acid content 0.5 M and 1 M, respectively. In addition, the data from XRD showed α-Al2O3 and t-ZrO2 phase can be formed at 1100°C with 1 M oxalic acid content. Transmission electron microscope (TEM) micrograph of calcined powders revealed as the oxalic acid content in the precursor solutions is increased from 0.25 M to 0.5 M concentration. The obtained materials could be modified from segregated nanoparticles to agglomerated nanoparticles and finally to large agglomerate with 1 M concentration of oxalic acid. The Fourier transform infrared spectra (FTIR) confirms the formation of α-Al2O3 in corroboration with X-ray studies." @default.
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- W1999462910 date "2008-10-30" @default.
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- W1999462910 title "Synthesis and Characterization of Alumina–Zirconia Nanopowders via an Oxalate Route" @default.
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- W1999462910 doi "https://doi.org/10.1080/10426910802382049" @default.
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