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• W1999616105 abstract "Hexagonal mesoporous titanosilicates with distinguishable framework charges and textural mesoporosity, namely, Ti-MCM-41 and Ti-HMS, were prepared at ambient temperature by electrostatic and neutral assembly processes, respectively. Titanium incorporation at the 2 mol % level for both materials was accompanied by increases in lattice parameters and wall thicknesses, but the framework pore sizes remained unaffected. Cross-linking of the anionic framework of as-synthesized Ti-substituted MCM-41 prepared by electrostatic S+I- and S+X-I+ assembly pathways (where S+ is a quaternary ammonium surfactant and I- and I+ are ionic silicon precursors) was enhanced significantly by Ti substitution, as judged by 29Si MAS NMR. The neutral framework of as-synthesized Ti-HMS formed by S°I° assembly (where S° is a primary amine and I° is a neutral silicon precursor) exhibited the same high degree of cross-linking as the unsubstituted silica analog. UV−vis and XANES spectra for the calcined forms of Ti-MCM-41 and Ti-HMS ind..." @default.
• W1999616105 created "2016-06-24" @default.
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• W1999616105 date "1996-01-01" @default.
• W1999616105 modified "2023-10-17" @default.
• W1999616105 title "Mesoporous Titanosilicate Molecular Sieves Prepared at Ambient Temperature by Electrostatic (S⁺I^-, S⁺X^-I⁺) and Neutral (S°I°) Assembly Pathways: A Comparison of Physical Properties and Catalytic Activity for Peroxide Oxidations" @default.
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• W1999616105 doi "https://doi.org/10.1021/ja960594z" @default.
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