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- W1999702926 abstract "Crystalline 1,3,4,5-tetra-O-acetyl-6-bromo-6-deoxy-keto-d-fructose was prepared by reaction of 1,3,4,5-tetra-O-acetyl-d-fructopyranose with triphenylphosphane dibromide in dichloromethane. Subsequent deprotection followed by reaction of the free 6-bromodeoxyfructofuranose with sodium azide in N,N-dimethylformamide furnished the corresponding 6-azidodeoxyketose. Catalytic hydrogenation led to 1-deoxymannojirimycin in 27% overall yield from 1,3,4,5-tetra-O-acetyl-d-fructopyranose. This access is simple, inexpensive, high-yielding and clearly suitable for multigram preparations." @default.
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- W1999702926 date "2002-02-01" @default.
- W1999702926 modified "2023-09-27" @default.
- W1999702926 title "A simple access to the d-mannosidase inhibitor, 1-deoxymannojirimycin" @default.
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- W1999702926 doi "https://doi.org/10.1016/s0008-6215(01)00291-9" @default.
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