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• W1999768839 abstract "The ability of pyrazolato ligands to form dinuclear complexes has been used to prepare a family of rhodium(I) complexes of the type [Rh(μ-pzFc)(L2)]2 (L2=2,5-norbornadiene (NBD) (1); 1,5-cyclooctadiene (COD) (2); 2CO (3)) containing ferrocenylpyrazolate (pzFc) as a bridging ligand. The diolefinic compounds 1 and 2 were obtained as the head-to-tail (H-T) isomer, whereas the tetracarbonyl derivative 3 was formed as a mixture of the head-to-tail (H-T) and head-to-head (H-H) isomers, as deduced by NMR studies in solution. The crystal structure determination of [Rh(μ-pzFc)(COD)]2 confirmed its identity as the H-T isomer having the boat conformation for the six-membered Rh(NN)2Rh ring in the solid state. Important structural parameters were Rh⋯Rh and Rh⋯H10 distances of 3.189(1) and 2.877 Å, respectively, according to the presence of weak intermolecular interactions. Electronic and electrochemical studies were also performed." @default.
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• W1999768839 date "1999-06-01" @default.
• W1999768839 modified "2023-10-18" @default.
• W1999768839 title "Ferrocenylpyrazolyl bridging rhodium dimers. Crystal structure of [Rh(μ-pzFc)(COD)]2" @default.
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• W1999768839 doi "https://doi.org/10.1016/s0022-328x(99)00006-6" @default.
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