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- W1999851312 abstract "In a simple reaction between Silver nitrate and Thiourea under the presence of Chitosan, novel fork architectures of silver sulfide (Ag 2 S) were obtained through In-situ self-assembly of Ag 2 S nanoparticles inside Chitosan matrix in aqueous basic environment. Samples were characterized by SEM, TEM, XRD, FTIR, Raman Spectroscopy and UV-vis Spectroscopy. Average particle size was found to be 8 nm from TEM analysis. Formation of crystalline monoclinic α-Ag 2 S was confirmed by SAED and X-ray diffraction analysis. The experimental results show that the fork architectures of Ag 2 S can be obtained from Tape like assemblies of Ag 2 S nanoparticles at the later stage of their growth with temperature. Raman spectra confirm the incorporation of Ag 2 S nanoparticles inside Chitosan matrix. Multiple resonant Raman peaks indicates that the yielded Ag 2 S nanoparticles possess good optical quality and crystalinity. FTIR spectra indicates that the Ag + ion is coupled with the C=O bond of the Chitosan molecules through the electrostatic interaction. UV-vis absorption spectrum of the Ag 2 S Fork architectures has a broad absorption band in the UV to visible region, and the blue-shifting of the band is observed along with the presence of both direct and indirect band gap." @default.
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- W1999851312 date "2012-05-01" @default.
- W1999851312 modified "2023-10-06" @default.
- W1999851312 title "Novel Fork Architectures of Ag<sub>2</sub>S Nanoparticles Synthesized through <i>In Situ</i> Self-Assembly inside Chitosan Matrix" @default.
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- W1999851312 doi "https://doi.org/10.4028/www.scientific.net/nh.1.23" @default.
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