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• W1999973531 abstract "Abstract The reactions of the heteroleptic zirconium diisopropoxide bis(acetylacetonate) in benzene solution with two equivalents of oximes, alkoxyalkanols, triphenylsilanol and trimethylsilyl acetate yield products with the formula [{MeC(O)CHC(O)Me} 2 ZrL 2 ] with L = —ONC(Me)C 5 H 4 N‐2, —ONC(Me)C 4 H 3 O‐2, —OCH 2 CH 2 OR (R = Me, Et, Bu n ; py = pyridine, fu = furan), —OSiPh 3 and —OSiMe 3 . Most of these derivatives are solids, but the [(acac) 2 Zr(OSiMe 3 ) 2 ] is a viscous oil. They could be purified either by recrystallization or by vacuum distillation; all of these are monomeric in boiling benzene. Their elemental analyses, molecular weight measurements and IR as well as NMR spectra were measured. The oximato complex [(acac) 2 Zr{ONC(Me)py‐2} 2 ] has been shown by single crystal X‐ray crystallography to be monoclinic and mononuclear in the solid state, where zirconium has the coordination number 8; all the ligands are situated in cis‐ position and the oximato ligand binds via N and O in a dihapto ( η 2 ‐N, O) manner." @default.
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• W1999973531 date "2003-12-01" @default.
• W1999973531 modified "2023-10-18" @default.
• W1999973531 title "Heteroleptic Complexes of Zirconium Acetylacetonates: Better Precursors for the Preparation of Zirconia. Structural Characterization of [(acac)2Zr{ONC(Me)py-2}2]" @default.
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• W1999973531 doi "https://doi.org/10.1002/zaac.200300310" @default.
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