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• W2000116514 abstract "The NPy···HNamide hydrogen bonding within the macrocyclic cavities in 9, 10, and 13 invokes their symmetrical electron-deficient structures (1H NMR) and consequently bind with water. This results in their poor ionophore characters. The steric requirement of methyl/benzyl substituents on amide N in 11 and 12 takes the substituents out of the cavity and thus positions the amide O toward the cavity (1H, 13C NMR and X-ray analysis). This arrangement of two pyridine N and two amide O (13C NMR, IR) binding sites provides an appropriate environment for selective binding toward Ag+ over Pb2+, Tl+, alkali, and alkaline earth cations. The increased spacer length in 14 leads to a lop-sided twist of pyridine rings (X-ray) and disturbs the above arrangement and leads to its poor binding character." @default.
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• W2000116514 date "1996-01-01" @default.
• W2000116514 modified "2023-10-18" @default.
• W2000116514 title "Synthetic Ionophores. 13. Pyridine−Diamide−Diester Receptors: Remarkable Effect of Amide Substituents on Molecular Organization and Ag⁺ Selectivity" @default.
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• W2000116514 doi "https://doi.org/10.1021/jo960859s" @default.
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