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- W2000168497 abstract "Photoreduction of Fe(OEP) (OEP: octaethylporphyrin) in organic solvents by visible light was demonstrated to be a ligand-aided process in which simultaneous coordinations of a base such as 2-methylimidazole (2MeIm) and of an aliphatic alcohol to two axial positions of the iron ion were required. Coordination of an alcohol was evidenced from the observation of the Fe–alcohol stretching (νFe–alcohol) resonance Raman (RR) band. Since this band exhibited an appreciable frequency shift between ROH and ROD, coordination of the alcohol in a protonated form was suggested. When a primary or secondary alcohol was added to the CH2Cl2 solution of FeIII (OEP)Cl in the presence of 2MeIm, a new absorption band appeared around 560–590 nm and the νFe–alcohol RR band was most intense for excitation at the maximum of the new absorption band. The new absorption was therefore assigned to the alcohol to FeIII charge transfer (CT) band. A tertiary alcohol gave neither the CT band nor the νFe–alcohol RR band, although some spect..." @default.
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- W2000168497 date "1991-08-01" @default.
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- W2000168497 title "Resonance Raman Study on Phot on eduction of Iron–Porphyrins. A Novel Insight into the Ligand-Aided Process" @default.
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