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- W2000192034 abstract "Titania was synthesized on a laboratory scale by the sol-gel method. Titania-based reversed-phase packings were prepared by reaction with octadecyltriethoxysilane. The titania and octadecyl-modified titanias obtained were tested under normal- and reversed-phase conditions to assess the influence of the titania matrix on retention. In normal-phase chromatography, the titania showed basic properties and strongly retained an acidic analyte. The k′ value of the acidic analyte decreased with increasing surface coverage because the influence of the titania matrix on retention was greatly reduced by octadecyl modification. In reversed-phase chromatography with the use of a mobile phase containing acetic acid-sodium acetate buffer, the titania behaved as an anion exchanger, and the influence of the titania matrix on retention was reduced because octadecyl modification decreased the number of anion-exchange sites. On the other hand, cation-exchange properties of titania were not detectable although benzylamine was retained. Octadecyl modification increased the retention of benzylamine by the formation of silanol and octadecyl groups." @default.
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- W2000192034 date "1996-01-01" @default.
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- W2000192034 title "Influence of titania matrix on retention behaviour in reversed-phase liquid chromatography" @default.
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- W2000192034 doi "https://doi.org/10.1016/0021-9673(95)00456-4" @default.
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