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- W2000197906 abstract "[reaction: see text] In the present investigation, solid-supported peptide olefins were converted quantitatively to aldehydes via the OsO(4)-NaIO(4)-mediated oxidative cleavage reaction. Addition of DABCO was essential to efficiently suppress the formation of hydroxymethyl ketone side products. The generated aldehydes were used in intramolecular N-acyliminium Pictet-Spengler reactions to produce highly pure pyrroloisoquinoline derivatives. The methodology was extended to allylglycine derivatives to enable the incorporation of pyrroloisoquinoline scaffolds within peptides." @default.
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- W2000197906 date "2005-05-28" @default.
- W2000197906 modified "2023-10-16" @default.
- W2000197906 title "Highly Efficient Solid-Phase Oxidative Cleavage of Olefins by OsO<sub>4</sub>−NaIO<sub>4</sub> in the Intramolecular <i>N</i>-Acyliminium Pictet−Spengler Reaction" @default.
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- W2000197906 doi "https://doi.org/10.1021/ol050870r" @default.
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