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• W2000201616 abstract "A detailed comparison of the proton conductivity of three highly ordered mesoporous silica host materials with large inner surface (Si-MCM-41, Si-SBA-15, Si-SBA-16) functionalised with sulfonic acid groups, which were obtained by anchoring and oxidation of thiol groups, is presented. The samples were characterised by X-ray diffraction, nitrogen adsorption, electron microscopy, FT-infrared spectroscopy and TGA/DTA measurements. The proton conductivity is deduced from impedance spectra taken in the temperature range 60–140 °C. All materials show strong dependence of the proton conductivities on the relative humidity, the degree of functionalisation and the pore geometry parameters. Whereas Si-SBA-16 composite materials are poor proton conductors due to the non-directed cubic 3D pore arrangement, functionalised Si-SBA-15 and Si-MCM-41 with hexagonal 1D pore channels exhibit promising proton conductivities at temperatures above 100 °C. For Si-MCM-41 the higher water storage capability is of additional advantage." @default.
• W2000201616 created "2016-06-24" @default.
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• W2000201616 date "2007-02-01" @default.
• W2000201616 modified "2023-09-25" @default.
• W2000201616 title "Proton conductivity of sulfonic acid functionalised mesoporous materials" @default.
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• W2000201616 doi "https://doi.org/10.1016/j.micromeso.2006.08.037" @default.
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