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- W2000207597 abstract "A detailed 91Zr NMR investigation is presented of the five component (cubic, monoclinic, tetragonal, orthorhombic and δ) phase mixture in the transformation toughened engineering ceramic, magnesia-partially-stabilised zirconia (MgPSZ). The phases are distinguished on the basis of the quadrupole interaction displayed in the powder pattern of the 91Zr (1/2, −1/2) transition. This paper reports: (i) the first characterisation of the magnesia-fully-stabilised cubic phase at the eutectic composition (13.5 mol% MgO); (ii) the observation of a poorly ordered tetragonal phase on fast cooling ZrO2 (9.3 mol% MgO) from the cubic phase field at 1720°C, and the subsequent growth and ordering of the tetragonal phase precipitates due to further annealing; (iii) the observation of the (partial) transformation of the cubic phase to the ordered δ-phase (Mg2Zr5O12) on annealing MgPSZ at 1100°C for 8 h; and (iv) the observation of the transformation of the tetragonal phase into the orthorhombic phase after cooling in liquid nitrogen, and the reverse transformation after heating to 600°C." @default.
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- W2000207597 date "1992-11-01" @default.
- W2000207597 modified "2023-09-27" @default.
- W2000207597 title "91Zr NMR characterisation of phases in transformation toughened zirconia" @default.
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- W2000207597 doi "https://doi.org/10.1016/s0926-2040(10)80001-3" @default.
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