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- W2000208260 abstract "Addition of 10 mol-% of diphenyl diselenide to hydrostannylation reactions involving electron-rich olefins results in a dramatic improvement in yield. For example, reaction of α-{[(tert-butyl)dimethylsilyl]oxy}styrene (1) with triphenylstannane (2a; 1.1 equiv.) in the presence of PhSeSePh and 2,2′-azobis[2-methylpropanenitrile] (AIBN) affords {2-{[(tert-butyl)dimethylsilyl]oxy}-2-phenylethyl}triphenylstannane (3a) in 95% yield after 2 h. This reaction presumably benefits, by the increased rate of H-atom transfer, from the in situ generated polarity-reversal catalyst, benzeneselenol." @default.
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- W2000208260 date "2006-10-01" @default.
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- W2000208260 title "Polarity-Reversal-Catalyzed Hydrostannylation Reactions: Benzeneselenol-Mediated Homolytic Hydrostannylation of Electron-Rich Olefins" @default.
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