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• W2000253337 abstract "The tricyclic ketone 19, an advanced intermediate in Aube's recently reported synthesis of aspidospermidine (4), is prepared in twelve steps from pyrrole (3). The key transformations involve a previously described intramolecular Michael addition reaction of pyrrole 10 and intramolecular Friedel–Crafts type cyclisation of the derived carboxylic acid 15 to ketone 16. Careful hydrogenation of this last compound afforded the fully saturated alcohol 17 which was readily oxidised to the target ketone 19." @default.
• W2000253337 created "2016-06-24" @default.
• W2000253337 creator A5034973943 @default.
• W2000253337 creator A5089692138 @default.
• W2000253337 date "2002-01-01" @default.
• W2000253337 modified "2023-09-27" @default.
• W2000253337 title "Exploiting multiple nucleophilic sites on pyrrole for the assembly of polyheterocyclic frameworks: application to a formal total synthesis of (±)-aspidospermidine" @default.
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• W2000253337 doi "https://doi.org/10.1039/b208821e" @default.
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