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- W2000253886 abstract "Abstract The separation of 12-molybdophosphoric Acid (12-MPA) from 12-molybdosilicic (12-MSA) acid by reverse phase liquid chromatography is described with UV-visible detection. The system utilizes a commercially available styrene-divinylbenzene column (Hamilton PRP-1) and a acetonitrile-water mobile phase which is 0.1 F in HCLO4 and 1.2 × 10−2 in molybdate ion. In solutions with acetonitrile concentrations of between 30 and 35% (V/V), 12-MPA is completely retained on the column and 12-MSA has a capacity factor between 1.2 and .6. In solutions with acetonitrile concentrations of between 50 and 60% (V/V) 12-MSA is unretained and 12-MPA has a capacity factor between 2.2 and 1.6. The detection limit is 5 × 10−7 M phosphate or silicate anion in 100 uL of injected sample. The linear dynamic range extends to 1.3 × 10−5 M for either anion. The relative standard deviation of the technique at the 5 × 10−6 M level is 2% for both silicate and phosphate. The analysis of phosphate in silicate rock is described." @default.
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- W2000253886 date "1989-03-01" @default.
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- W2000253886 title "The Separation of 12-Molybdophosphoric Acid from 12-Molybdosilicic Acid by Reverse Phase Liquid Chromatography" @default.
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- W2000253886 doi "https://doi.org/10.1080/01483918908051743" @default.
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