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- W2000269027 abstract "The total synthesis of hyptolide, a naturally occurring α,β-unsaturated six-membered δ-lactone substituted with a polyoxygenated chain, is described. Sharpless kinetic resolution and opening of two different epoxy alcohols under two different conditions—Swern oxidation conditions and a radical reaction using Cp2TiCl—fixed the stereocenters at C-9, C-11, and C-12, respectively. Brown’s asymmetric allylation reaction installed the remaining stereocenter at C-6. A RCM protocol was used for construction of the α,β-unsaturated six-membered δ-lactone moiety of the molecule." @default.
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- W2000269027 date "2008-09-01" @default.
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- W2000269027 title "Total synthesis of hyptolide" @default.
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- W2000269027 doi "https://doi.org/10.1016/j.tetlet.2008.07.033" @default.
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