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- W2000281054 abstract "Ti3AIC2 has good oxidation resistance at high temperatures owing to the formation of protective Al2O3 layer. However, as it is directly exposed to air at 500 °C and especially 600 °C, the scales formed on Ti3AIC2 exhibits poor protectivity because of the oxidation-induced microcracks, which limits the potential application of this technologically important material. In this work, the oxidation resistance of Ti3AIC2 at 500 °C and 600 °C was significantly improved by pre-oxidation at 1000–1300 °C for a short time of 2 h in air. The oxidation of the pre-oxidized Ti3AIC2 at 600 °C generally obeyed a parabolic rate law instead of the speed-up linear relation in the case without pre-oxidation. As revealed by X-ray diffraction, Raman spectroscopy results and SEM observations, the remarkable improvement of oxidation resistance after pre-oxidation was attributed to the protective layers formed on Ti3AIC2 during pre-oxidation, which inhibited the formation of anatase TiO2 that resulted in the oxidation-induced microcracks. Moreover, this work confirmed that the mechanism proposed previously for the anomalous oxidation of Ti3AIC2 in air at 500–600 °C was correct." @default.
- W2000281054 created "2016-06-24" @default.
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- W2000281054 date "2003-08-01" @default.
- W2000281054 modified "2023-09-24" @default.
- W2000281054 title "Improvement of intermediate-temperature oxidation resistance of Ti3AIC2 by pre-oxidation at high temperatures" @default.
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- W2000281054 doi "https://doi.org/10.1007/s10019-003-0252-4" @default.
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