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W2000294286 abstract "Neutral lead complexes of a series of phosphorylarenethiol and thiophosphorylarenethiol proligands have been synthesised. Compounds [Pb{2-(Ph2P)C6H4S}2] 1, [Pb{2-(Ph2P)-6-(Me3Si)C6H3S}2] 2 and [Pb{2-(Ph2PO)-6-(Me3Si)C6H3S}2] 3 were obtained by the electrochemical oxidation of a lead anode in a cell containing an acetonitrile solution of the ligand. [Pb{2-(Ph2P(O)CH2)C6H4S}2] 4, [Pb{2-(Ph2P(S)CH2)C6H4S}2] 5 and [Pb{2,6-(Ph2P(S)CH2)2C6H3S}2] 6 were obtained by addition of the appropriate proligand to a methanol solution of lead acetate. The molecular structures of 3, 4 and 5 show the metal in a five-coordinate geometry with the stereochemically active lone pair on Pb(II) in an equatorial position of a trigonal bipyramid. In 3, the metal coordination is supplemented by an additional weak Pb–(η6-C6H6) intermolecular interaction with a phenyl ring from a neighbouring molecule. Compound 6 consists of monomeric neutral molecules with the lead atom in a pseudo trigonal-bipyramidal geometry and additional weak intramolecular coordination with two sulfur atoms." @default.
W2000294286 created "2016-06-24" @default.
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W2000294286 date "2000-01-01" @default.
W2000294286 modified "2023-10-18" @default.
W2000294286 title "Lead(II) complexes with phosphorylthiolato and thiophosphorylthiolato ligands" @default.
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W2000294286 doi "https://doi.org/10.1039/a908496g" @default.
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