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- W2000298997 abstract "Abstract Oxiranecarbaldimines 1 , which are easily accessible in a two‐step procedure, were converted into [1,4]dithiepino[2,3‐ b ]furans 5 by the addition of lithiated 1,3‐dithiane and subsequent aqueous workup under acidic conditions. In case of bis(imine) 6 , the isolation of the intermediate bis(aziridinyl alcohol) 7 was possible and resulted from an aza‐Payne rearrangement. Acid treatment of 7 led to the bis(furan) 8 . According to quantum chemical calculations, the key step of the acid‐catalyzed step is the ring expansion of the 1,3‐dithiane with simultaneous ring opening of the aziridine. Several [1,4]dithiepino[2,3‐ b ]furan derivatives 5 and 8 were characterized by X‐ray diffraction." @default.
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- W2000298997 date "2011-12-12" @default.
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- W2000298997 title "[1,4]Dithiepino[2,3‐<i>b</i>]furans from Oxiranecarbaldimines and Lithiated 1,3‐Dithiane: A Series of Rearrangement Reactions in One Pot" @default.
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- W2000298997 doi "https://doi.org/10.1002/ejoc.201101323" @default.
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