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• W2000301942 abstract "The recently discovered intramolecular aza-xylylene Diels–Alder reaction, based on a 1,4-dehydrohalogenation reaction, was extended in terms of substrates and leaving groups allowing the assembly of tetrahydroquinolines in two synthetic steps. Intramolecular cleavage of a thiocarbamate using triphenylphosphine and tetrachloromethane (Appel conditions) to give chloromethyl phenylisocyanate has been presented for the first time. The synthetic feasibility of this process was demonstrated in the first total syntheses of the alkaloids rac-Angustureine and 1-methyl-2-propyltetrahydroquinoline." @default.
• W2000301942 created "2016-06-24" @default.
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• W2000301942 date "2003-08-01" @default.
• W2000301942 modified "2023-09-24" @default.
• W2000301942 title "The aza-xylylene Diels–Alder approach for the synthesis of naturally occurring 2-alkyl tetrahydroquinolines" @default.
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• W2000301942 doi "https://doi.org/10.1016/s0040-4020(03)00915-3" @default.
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