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- W2000321199 abstract "A method is described for the selective determination of lead in paper chromatograms, down to 1 μg (standard deviation 11%). After development and drying, the lead spot is sprayed with a Na2H32PO4 solution and dried. Excess reagent and alkaline earth phosphates are eluted with a borax—oxalate buffer of ph 8.0. Eventually, the radio-activity of the lead spot is measured. The filter paper renders the method about 40 times more sensitive than existing radiometric techniques with phosphate-32P. The method can be modified for the simultaneous determination of many cations. Une méthode radiométrique est proposée pour le dosage du plomb par chromatographie sur papier, au moyen de phosphate disodique, marqué au phosphore-32. La sensibilité est meilleure que celle obtenue avec les autres techniques radiométriques, à l'aide de Na2H32PO4. Beschreibung einer radiometrischen Methode zur Bestimmung von Spuren von Blei durch Papierchromatographie unter Verwendung von Dinatriumphosphat-32P. Auf mögliche Modifikationen zur gleichzeitigen Bestimmung mehrerer Kationen wird hingewiesen." @default.
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- W2000321199 date "1961-12-01" @default.
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- W2000321199 title "Radiometric trace analysis quantitative paper chromatography of lead with phosphate-32P" @default.
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- W2000321199 doi "https://doi.org/10.1016/0003-2670(61)80136-0" @default.
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