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• W2000347617 abstract "Abstract The 60 MHz 1NMR spectra of racemic metapramine, l, have been studied in CDCl3 solution at 28° with the achiral shift reagent, tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato) europium(III), 2, and the chiral reagent, tris[3-(heptafluoropropylhydroxy-methylene)-d-camphoratoleuropium(III), 3. Reagent 2 additions resulted in changes of the apparent vicinal coupling constants within the CH-CH2 moiety, as observed from the NCH methine resonance. The chiral 3 led to observable enantiomeric shift differences for the 2° NCH3 signal that could have potential for direct optical purity determinations of 1. Results with 2 and 3 are interpreted as consistent with major shift reagent binding at the 2° nitrogen, with conformer equilibria changes sterically induced by this complexation." @default.
• W2000347617 created "2016-06-24" @default.
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• W2000347617 date "1987-01-01" @default.
• W2000347617 modified "2023-09-25" @default.
• W2000347617 title "1H NMR Spectral Simplification with Achiral and Chiral Lanthanide Shift Reagents. Metapramine. Variation of Coupling Constants Produced by Shift Reagent" @default.
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• W2000347617 doi "https://doi.org/10.1080/00387018708081601" @default.
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