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- W2000357624 abstract "Bulk nanocrystalline selenium (nc-Se) samples were prepared by crystallizing as-quenched amorphous selenium (a-Se). The structure of nc-Se was investigated by x-ray diffraction (XRD) and transmission electron microscopy (TEM). nc-Se samples are of trigonal structure with grain sizes ranging from 8.4 to 27.8 nm. Direct TEM observations showed that nc-Se consists of lamellae which are made up of fibres with a nanometre-sized thickness. A lattice distortion was revealed in nc-Se from quantitative XRD measurements, i.e., the lattice parameter a increases and c decreases simultaneously with a reduction in grain size. For the samples with grain sizes smaller than 12 nm, the unit cell volume is expanded; but it is contracted for those with grain sizes larger than 12 nm. A change of elastic modulus with grain size is inferred from the change of unit cell volume." @default.
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- W2000357624 date "1995-07-03" @default.
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- W2000357624 title "Structural characteristics and lattice distortion of nanocrystalline selenium" @default.
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- W2000357624 doi "https://doi.org/10.1088/0953-8984/7/27/017" @default.
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