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- W2000365723 abstract "Abstract Monomeric titanatrane i-PrOTi(OCMe2CH2)3N (1) and dimeric titanatranes [i-PrOTi(OCH2CH2)nN(CH2CMe2O)3−n]2 (n = 1, 2; n = 2, 3) were synthesized by the reaction of Ti(O-i-Pr)4 with a series of triethanolateamines such as (OCH2CH2)nN(CH2CMe2O)3−n3− (n = 0, Lig1; n = 1, Lig2; n = 2, Lig3), which vary by the number of CMe2 groups adjacent to a OH functionality from 3 (Lig1H3) to 2 (Lig2H3) to 1 (Lig3H3). The resultant titanatranes 1–3 have been characterized by solution 1H and 13C{1H} NMR and their solid state structures have been determined by X-ray crystallography. Whereas compound 1 is monomeric in the solid state, compounds 2 and 3 are dimeric, due to the reduction of the steric congestion in the vicinity of the Ti." @default.
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- W2000365723 date "2010-01-01" @default.
- W2000365723 modified "2023-10-16" @default.
- W2000365723 title "Selective synthesis of monomeric or dimeric titanatranes via fine tuning in triethanolateamine ligand" @default.
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- W2000365723 doi "https://doi.org/10.1016/j.poly.2009.06.017" @default.
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