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- W2000375913 abstract "Total syntheses of circumdatin F and circumdatin C, which both possess a 3H-quinazolin-4-one as well as a 1,4-benzodiazepin-5-one moiety, are described. A tripeptide derivative was synthesized as a key intermediate and dehydrated to a benzoxazine by reaction with triphenylphosphine, iodine, and a tertiary amine. The natural products were attained via rearrangements to an amidine intermediate, deprotection with 45% HBr in acetic acid, and cyclization on silica gel." @default.
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- W2000375913 date "2001-03-22" @default.
- W2000375913 modified "2023-10-10" @default.
- W2000375913 title "Total Syntheses of the Benzodiazepine Alkaloids Circumdatin F and Circumdatin C" @default.
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- W2000375913 doi "https://doi.org/10.1021/jo001696h" @default.
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