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• W2000416239 abstract "The cyclic disilane amidinium salt [(Me2SiNDipp)2CH]OTf (Dipp = 2,6-iPr2C6H3; OTf = OSO2CF3−) was obtained in high yield, and attempts to generate the N-heterocyclic carbene [(Me2SiNDipp)2C:] via deprotonation with numerous bases exclusively gave ring-opened products of the general form: R–SiMe2–SiMe2N(Dipp)–CHNDipp (R = carbon-, nitrogen- or oxygen-based nucleophiles). Although this approach was not directly successful in generating silicon-based N-heterocyclic carbenes, judicious manipulation of the ring-bound substituents might enable the future synthesis of new inorganic carbenes to transpire." @default.
• W2000416239 created "2016-06-24" @default.
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• W2000416239 date "2013-09-01" @default.
• W2000416239 modified "2023-09-24" @default.
• W2000416239 title "Preparation of a stable disilane amidinium heterocycle and attempted syntheses of an inorganic N-heterocyclic carbene" @default.
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• W2000416239 doi "https://doi.org/10.1016/j.jorganchem.2013.04.029" @default.
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