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- W2000451942 abstract "2-O-Acetyl-1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose and 1,6-anhydro-3,4-O-isopropylidene-2-O-methylthiomethyl-β-D-galactopyranose were identified as by-products in the methyl sulphoxide-acetic anhydride oxidation of 1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose to 1,6-anhydro-3,4-O-isopropylidene-β-D-lyxo-hexopyranosulose (isolated as the stable 2,2-gem-diol derivative). Syntheses of 1,6-anhydro-3,4-O-isopropylidene-2-O-methyl-β-D-talopyranose and 1,6-anhydro-2-O-methyl-β-D-talopyranose from 1,6-anhydro-3,4-O-isopropylidene-β-D-talopyranose are described. The former compound exhibited unusual chromatographic behaviour. 1,6-Anhydro-2,3-O-isopropylidene-β-D-talopyranose was isolated from an incomplete hydrolysis of 1,6-anhydro-3,4-O-isopropylidene-β-D-talopyranose to 1,6-anhydro-β-D-talopyranose, indicating that acetal migration was accompanying hydrolysis. The 2,3-acetal was the major product of reaction of acetone with 1,6-anhydro-β-D-talopyranose in the presence of sulphuric acid." @default.
- W2000451942 created "2016-06-24" @default.
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- W2000451942 date "1968-08-01" @default.
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- W2000451942 title "Further observations on derivatives of 1,6-anhydro-β-D-talopyranose; an example of acetal migration accompanying hydrolysis" @default.
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- W2000451942 doi "https://doi.org/10.1016/s0008-6215(00)82967-5" @default.
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