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• W2000471229 abstract "A new class of organic–inorganic hybrid porous clay heterostructures (HPCHs) have been prepared through the surfactant-directed assembly of organosilica in the galleries of montmorillonite. The reaction involved hydrolysis and condensation of phenyltriethoxysilane and tetraethoxysilane in the presence of intragallery surfactant templates (dodecylame and cetyltrimethylammonium ion). The surfactant templates were removed from the pores by solvent-extraction. The products were characterized by X-ray diffraction (XRD), N2 adsorption, solid-state 29Si and 13C NMR, and FTIR. XRD patterns indicated a regular interstratification of the clay layers for HPCHs. Depending on loading of phenyl groups, HPCHs had BET surface areas of 390–771 m2 g−1, pore volumes of 0.3–0.59 cm3 g−1, and the framework pore sizes in the supermicropore to small mesopore range (1.2–2.6 nm). HPCHs were hydrophobic and acidic." @default.
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• W2000471229 date "2004-02-01" @default.
• W2000471229 modified "2023-09-28" @default.
• W2000471229 title "Novel acidic porous clay heterostructure with highly ordered organic–inorganic hybrid structure: one-pot synthesis of mesoporous organosilica in the galleries of clay" @default.
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• W2000471229 doi "https://doi.org/10.1016/j.micromeso.2003.11.002" @default.
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