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- W2000472925 abstract "Die Anwendung der 1H{2H} Off-Resonance Rauschentkopplung führt in den 1H-NMR-Spektren nicht vollständig deuterierter Verbindungen zu einer selektiven Verbreiterung der Protonenrestsignale, sofern diese durch H/D Kopplungen aufgespalten sind. Diese Entkopplungstechnik ermöglicht den einfachen Nachweis von Signalen, die von Lösungsmittelrestsignalen verdeckt sind, wie am Beispiel von Gemischen aus Aceton und Aceton-d6 gezeigt wird. Typische Geräteparameter zur experimentellen Durchführung dieser Doppelresonanztechnik werden angegeben. 1H {2H} off-resonance noise decoupling experiments with incompletely deuterated compounds result in a selective broadening of those residual proton signals which are split by H/D couplings. By this technique hidden resonance lines which are overlapped by solvent signals can be easily detected, as is demonstrated by the analysis of acetone/acetone-d6 mixtures. Typical experimental details are given." @default.
- W2000472925 created "2016-06-24" @default.
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- W2000472925 date "1977-07-01" @default.
- W2000472925 modified "2023-10-18" @default.
- W2000472925 title "Selektive Verbreiterung von1H-NMR Restsignalen deuterierter Lösungsmittel" @default.
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- W2000472925 doi "https://doi.org/10.1002/mrc.1270090709" @default.
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