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- W2000474493 abstract "The formation of Fmoc-L-Ala-L-Phlac-OBzl (and Fmoc-D-AIa-L-Phlac-OBzl if there is racemisation) has been monitored by HPLC analysis for a number of coupling conditions between Fmoc-L-AIa-OH and H-Phlac-OBzl. For this depside link formation it is revealed that CDI, DCC/DMAP and mixed anhydride couplings gave yields near to 50%. Couplings via TBTU, TNTU and TSTU gave lower yields. The best yields were achieved by acid chloride (61%), urethane-N-carboxyanhydrides (80%) and by PyBroP coupling (82%)." @default.
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- W2000474493 date "1995-01-01" @default.
- W2000474493 modified "2023-10-09" @default.
- W2000474493 title "A model reaction for assessing the coupling and chiral efficiency of reagents in depside bond formation" @default.
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- W2000474493 doi "https://doi.org/10.1039/p29950002335" @default.
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