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- W2000485547 abstract "► High surface area Mn 3 O 4 nanoparticles obtained by a solvent-free low temperature route. ► 3,6,9-Trioxadecanoic acid allows to obtain nanocrystalline hausmannite. ► Tape casted electrodes show up to 300 mAh g −1 capacity after more than 40 cycles at a C /3 rate. ► Upper cut off voltage strongly influences capacity retention upon cycling at high C rates. Nanocrystalline high surface area Mn 3 O 4 powder was obtained at low temperature by a solvent-free route. The precursor was a mixture of manganese (II) acetate, 3,6,9-trioxadecanoic acid (TODA) and ammonium acetate that were intimately mixed by grounding in an agate mortar. Nanocrystalline Mn 3 O 4 was obtained by thermal treatment at 120 °C. Powder X-ray diffraction, selected area electron diffraction, high resolution transmission electron microscopy, and Fourier transformed infrared characterization confirmed the formation of the hausmannite phase. The as-prepared mesoporous material has high specific surface area (120 m 2 g −1 ). The performances of tape casted Mn 3 O 4 nanopowder electrodes were investigated as anode material for lithium ion batteries. High capacity values were achieved at diverse C rates. Capacity fading was found to be dependent on the upper cut off voltage, the presence of a plateau at 2.25 V vs . Li + /Li being detrimental for long term cyclability." @default.
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- W2000485547 date "2012-09-01" @default.
- W2000485547 modified "2023-10-09" @default.
- W2000485547 title "High surface area nanocrystalline hausmannite synthesized by a solvent-free route" @default.
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- W2000485547 doi "https://doi.org/10.1016/j.materresbull.2012.05.050" @default.
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