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• W2000493978 abstract "The present work describes the development and optimization of a capillary (zone) electrophoresis/mass spectrometric (CE/MS) analysis method for polar hydrophilic aromatic sulfonates (ASs). The compounds were detected by negative ion electrospray ionization (NIESI) and selected ion monitoring (SIM). In comparison with CE/UV, for CE/MS a lower-concentration volatile ammonium acetate buffer (5 mM) without organic modifier and a higher separation voltage were better suited for separation. Sensitivity of CE/MS was slightly better than for CE/UV, with the limit of detection (LOD) ranging between 0.1 and 0.4 mg l−1. For verification of the CE/MS results, ASs were also analysed by ion-pair liquid chromatography/diode array UV detection coupled in series with electrospray mass spectrometry (IPC/DAD/ESI-MS). Real water samples of different waste water treatment plants (WWTPs) in Catalonia (NE Spain) were extracted by solid-phase extraction (SPE) with LiChrolut EN and analysed with CE/MS and LC/MS. ASs were found in influent and effluent water samples of the WWTPs in the µg l−1 concentration range. LC/MS offered a higher separation efficiency and sensitivity than CE/MS. Therefore with LC/MS more compounds could be identified in the WWTPs. The persistency of the ASs was distinct: some compounds were well degraded during the water treatment process, while others were quite persistent. Copyright © 2000 John Wiley & Sons, Ltd." @default.
• W2000493978 created "2016-06-24" @default.
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• W2000493978 date "2000-01-01" @default.
• W2000493978 modified "2023-10-15" @default.
• W2000493978 title "Analysis of polar hydrophilic aromatic sulfonates in waste water treatment plants by CE/MS and LC/MS" @default.
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• W2000493978 doi "https://doi.org/10.1002/1096-9888(200010)35:10<1197::aid-jms51>3.0.co;2-o" @default.
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