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• W2000524032 endingPage "3537" @default.
• W2000524032 startingPage "3528" @default.
• W2000524032 abstract "We have recorded 13C NMR spectra of several preparations of amorphous samples, V-amyloses and their hydrates to gain insight into their relative stability and subsequent hydration-induced conformational change. It was found that the 13C NMR line width of the iodine complex prepared as a precipitate in aqueous solution was the narrowest among these preparations, including the iodine complex formed from cast film. It is noteworthy that these V-amyloses are not always stable when they are equilibrated in an atmosphere of 96% R. H. in a desiccator and converted to B-type form, consistent with previous observation by Senti and Witnauer (J. Am. Chem. Soc., 70, 1438 (1948)). 2H NMR line shape and spin-lattice relaxation times were measured for partially deuterated V and B-type amylose samples containing DMSO-d6 and deuterium oxide, respectively, to explore the dynamics of the DMSO and water molecules bound to the polymer chains. It is unlikely that any drastic conformational change such as unfolding followed by ..." @default.
• W2000524032 created "2016-06-24" @default.
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• W2000524032 date "1991-12-01" @default.
• W2000524032 modified "2023-10-13" @default.
• W2000524032 title "Conformational Stability of V-Amyloses and Their Hydration-Induced Conversion to B-Type Form as Studied by High-Resolution Solid-State¹³C NMR Spectroscopy" @default.
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• W2000524032 doi "https://doi.org/10.1246/bcsj.64.3528" @default.
• W2000524032 hasPublicationYear "1991" @default.
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