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• W2000541750 endingPage "3407" @default.
• W2000541750 startingPage "3403" @default.
• W2000541750 abstract "The reaction of [Pd3(OAc)6] with (E)-acetophenone oxime and pyridine in CHCl3 under reflux affords the metallacycle [Pd(OAc){C,N-(C6H4C(CH3)NOH)-2}(py)] (1) as a yellow air-stable complex. The same reaction carried out at room temperature in the absence of pyridine affords the trinuclear oximato complex [Pd(μ-(E)-ONC(CH3)Ph)(μ-OAc)]3 (2), which can be converted into 1 upon heating in the presence of pyridine. As indicated by 1H and 31P NMR spectroscopy, complex 1 reacts with methylparathion in acetone-d6–D2O solutions to afford [Pd(SP(O)(OCH3)2){C,N-(C6H4C(CH3)NOH)-2}(py)] (3) and [Pd(μ-SP(O)(OCH3)2){C,N-(C6H4C(CH3)NOH)-2}]2 (4) as well as free p-nitrophenol. Compounds 1–4 have been characterized by single-crystal X-ray analysis, NMR and EA. Compounds 1 and 3 are mononuclear complexes with the acetate and dimethylthiophosphate ligand, respectively, trans from the phenyl group. Compound 2 is a trinuclear complex whose structure can be derived from that of [Pd3(OAc)6] by replacing three of the acetate ligands on one side of Pd3 plane by three N,O-coordinated oximate ligands. Complex 4 is a dinuclear complex in which the two square-planar palladium moieties are linked by the sulfur atoms of the bridging dimethylthiophosphate ligands." @default.
• W2000541750 created "2016-06-24" @default.
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• W2000541750 date "2004-01-01" @default.
• W2000541750 modified "2023-10-16" @default.
• W2000541750 title "Stoichiometric reactions of methylparathion with a palladium aryl oxime metallacycle" @default.
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• W2000541750 doi "https://doi.org/10.1039/b411313f" @default.
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