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- W2000547908 abstract "A reaction between vinyl chloride and the solvent (methanol) was observed during volatile organic compound (VOC) analysis on a gas chromatograph/quadrupole ion trap mass spectrometer (GC/MS). A chromatographic peak at a retention time consistent with vinyl chloride produced a mass spectrum without the characteristic chlorine isotope ions m/z 62 and 64 but instead contained an apparent molecular ion, m/z 58. The m/z 58 ion is not found in the reference spectrum of vinyl chloride. This spectrum was observed when methanol was used as solvent in internal standard, surrogate standard, or analyte solutions. Subsequent VOC standard analysis indicated that the abundance of the m/z 58 ion was directly proportional to the amount of vinyl chloride in the water samples. The correct spectrum for vinyl chloride was observed (m/z 62 and 64) when no methanol was added. From these experiments, we concluded that a reaction was occurring between the vinyl chloride and methanol in the ion trap producing a new species with a ..." @default.
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- W2000547908 date "1999-03-25" @default.
- W2000547908 modified "2023-09-27" @default.
- W2000547908 title "Reactions of Vinyl Chloride and Methanol in a Quadrupole Ion Trap Mass Spectrometer during VOC Analysis" @default.
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- W2000547908 doi "https://doi.org/10.1021/es980916u" @default.
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