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- W2000548818 abstract "The syntheses are described of ortho-metalated iridium arylhydrazido complexes [Ir(NHNHC6H3X)(CO)(PPh3)2]BF4, where X = H, 4-F, 3-F, 2-F, 4-OMe, 2-OMe, 2-NO2, 3-NO2, 3-CH3, 4-CH3 and 2-CF3 from the reactions of the corresponding arenediazonium tetrafluoroborates with IrH(CO)(PPh3)3 or IrH(CO)2(PPh3)2. A high-yield synthesis of the 2-NO2 complex from the diazonium salt and IrCl(CO)(PPh3)2 is also reported, and this complex has been the subject of a multinuclear (1H, 13C, 31P, 15N) NMR study. Oxidation of these arylhydrazido complexes to ortho-metalated aryldiazene complexes [Ir(NHNC6H3X)(Y)(CO)(PPh3)2]BF4, where Y = F, FBF3, Cl, Br or I occurs with air and halogens." @default.
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- W2000548818 date "1974-10-01" @default.
- W2000548818 modified "2023-09-26" @default.
- W2000548818 title "Reply to discussion" @default.
- W2000548818 doi "https://doi.org/10.1016/0020-7403(74)90104-0" @default.
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