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- W2000554562 abstract "Cementite dissolution in cold-drawn pearlitic steel (0.8 wt.% carbon) wires has been studied by quantitative X-ray diffraction (XRD) and Mössbauer spectroscopy up to drawing strain 1.4. Quantification of cementite-phase fraction by Rietveld analysis has confirmed more than 50% dissolution of cementite phase at drawing strain 1.4. It is found that the lattice parameter of the ferrite phase determined by Rietveld refinement procedure remains nearly unchanged even after cementite dissolution. This confirms that the carbon atoms released after cementite dissolution do not dissolve in the ferrite lattice as Fe-C interstitial solid solution. Detailed analysis of broadening of XRD line profiles for the ferrite phase shows high density of dislocations (∼1015/m2) in the ferrite matrix at drawing strain 1.4. The results suggest a dominant role of ⟨1 1 1⟩ screw dislocations in the cementite dissolution process. Post-deformation heat treatment leads to partial annihilation of dislocations and restoration of cementite phase. Based on these experimental observations, further supplemented by TEM studies, we have suggested an alternative thermodynamic mechanism of the dissolution process." @default.
- W2000554562 created "2016-06-24" @default.
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- W2000554562 date "2013-12-01" @default.
- W2000554562 modified "2023-09-26" @default.
- W2000554562 title "X-ray diffraction and Mössbauer spectroscopy studies of cementite dissolution in cold-drawn pearlitic steel" @default.
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- W2000554562 doi "https://doi.org/10.1080/14786435.2013.838010" @default.
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