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- W2000565342 abstract "The synthesis of enantiomerically pure, cyclic, γ,γ-difluorinated β-amino acids with various ring sizes has been carried out with a cross-metathesis (CM) reaction being one of the key steps, followed by a Dieckmann-type condensation to bring about the cyclization. Subsequent catalytic hydrogenation under microwave irradiation with (−)-8-phenylmenthol as a chiral auxiliary led to the successful chemo- and diastereoselective chemical reduction of the resulting cyclic β-enamino esters. The efficiency and scope of the CM reaction with different types of fluorinated imidoyl chlorides and unsaturated esters has also been studied in order to determine the optimal reaction conditions with regard to selectivity and reactivity." @default.
- W2000565342 created "2016-06-24" @default.
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- W2000565342 date "2009-04-06" @default.
- W2000565342 modified "2023-10-09" @default.
- W2000565342 title "Cross-Metathesis Reactions as an Efficient Tool in the Synthesis of Fluorinated Cyclic β-Amino Acids" @default.
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- W2000565342 doi "https://doi.org/10.1021/jo900296d" @default.
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