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- W2000585627 abstract "A continuous-flow protocol for the preparation of organic nitriles from carboxylic acids has been developed. The method is based on the acid–nitrile exchange reaction with acetonitrile, used as the solvent, and takes place without any catalyst or additives under the high-temperature/high-pressure conditions employed. At 350 °C and 65 bar, where acetonitrile is in its supercritical state, the transformation of benzoic acid to benzonitrile requires 25 min. The protocol has been tested for a variety of nitriles, including aromatic and aliphatic substrates." @default.
- W2000585627 created "2016-06-24" @default.
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- W2000585627 date "2013-10-08" @default.
- W2000585627 modified "2023-10-14" @default.
- W2000585627 title "Direct Preparation of Nitriles from Carboxylic Acids in Continuous Flow" @default.
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- W2000585627 doi "https://doi.org/10.1021/jo401945r" @default.
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