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• W2000619767 abstract "In this contribution, different amounts of nickel were incorporated into the mesopores of MCM-41 via an in situ approach. A hydrophobic nickel precursor was incorporated into the nanochannels of mesoporous silica by manipulation of solvent-solute interaction. The synthesized material was characterized using X-ray diffraction, nitrogen physisorption, temperature programmed reduction, and transmission electron microscopy. The results implicate the formation of MCM-41 with well-ordered hexagonal structure and establish also the presence of nickel nanoparticles inside the nanochannels of mesoporous silica. Adsorptive desulfurization of gas oil was conducted using the nickel-incorporated MCM-41 samples. The effects of nickel concentration, temperature of process and feed flow rate on the desulfurization process were examined. The MCM-41 containing 6 wt.% of nickel had both the highest breakthrough sulfur adsorption capacity and total sulfur adsorption capacity, which were 0.69 and 1.67 mg sulfur/g adsorbent, respectively. The breakthrough sulfur adsorption capacity was almost regained after reductive regeneration of spent adsorbent. The obtained results suggest that the method applied for the synthesis of Niy/MCM resulted in formation of well-dispersed, accessible and small nickel nanoparticles incorporated into the pores of MCM-41 which might be an advantage for adsorption of refractory sulfur compounds from low sulfur gas oil." @default.
• W2000619767 created "2016-06-24" @default.
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• W2000619767 date "2011-09-01" @default.
• W2000619767 modified "2023-09-23" @default.
• W2000619767 title "In situ incorporation of nickel nanoparticles into the mesopores of MCM-41 by manipulation of solvent–solute interaction and its activity toward adsorptive desulfurization of gas oil" @default.
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• W2000619767 doi "https://doi.org/10.1016/j.jhazmat.2011.06.089" @default.
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