Matches in SemOpenAlex for { <https://semopenalex.org/work/W2000632421> ?p ?o ?g. }
- W2000632421 abstract "A method was established for the determination of desipramine in biological samples using liquid-liquid-liquid microextraction followed by in-syringe derivatization and gas chromatography-nitrogen phosphorus detection. The extraction method was based on the use of two immiscible organic solvents. n-Dodecane was impregnated in the pores of the hollow fiber and methanol was placed inside the lumen of the fiber as the acceptor phase. Acetic anhydride was used as the reagent for the derivatization of the analyte inside the syringe barrel. Parameters that affect the extraction efficiency (composition of donor and acceptor phase, ionic strength, sample temperature, and extraction time) as well as derivatization efficiency (amount of acetic anhydride and reaction time and temperature) were investigated. The limit of detection was 0.02 μg/L with intra and interday RSDs of 2.6 and 7.7%, respectively. The linearity of the method was in the range of 0.2-20 μg/L (r(2) = 0.9986). The method was successfully applied to determine desipramine in human plasma and urine." @default.
- W2000632421 created "2016-06-24" @default.
- W2000632421 creator A5048729527 @default.
- W2000632421 creator A5051141279 @default.
- W2000632421 creator A5052534020 @default.
- W2000632421 creator A5065033176 @default.
- W2000632421 date "2012-08-09" @default.
- W2000632421 modified "2023-10-18" @default.
- W2000632421 title "Determination of desipramine in biological samples using liquid-liquid-liquid microextraction combined with in-syringe derivatization, gas chromatography, and nitrogen/phosphorus detection" @default.
- W2000632421 cites W1910943165 @default.
- W2000632421 cites W1915365545 @default.
- W2000632421 cites W1963621754 @default.
- W2000632421 cites W1971978841 @default.
- W2000632421 cites W1976973422 @default.
- W2000632421 cites W1984738696 @default.
- W2000632421 cites W1989077540 @default.
- W2000632421 cites W1990852254 @default.
- W2000632421 cites W1992773908 @default.
- W2000632421 cites W1997956721 @default.
- W2000632421 cites W2003100143 @default.
- W2000632421 cites W2005017007 @default.
- W2000632421 cites W2007229044 @default.
- W2000632421 cites W2007720743 @default.
- W2000632421 cites W2009167846 @default.
- W2000632421 cites W2016592208 @default.
- W2000632421 cites W2021066675 @default.
- W2000632421 cites W2021164986 @default.
- W2000632421 cites W2023587691 @default.
- W2000632421 cites W2028877450 @default.
- W2000632421 cites W2038492841 @default.
- W2000632421 cites W2040235588 @default.
- W2000632421 cites W2042639356 @default.
- W2000632421 cites W2045100458 @default.
- W2000632421 cites W2048669238 @default.
- W2000632421 cites W2048705571 @default.
- W2000632421 cites W2049076273 @default.
- W2000632421 cites W2054387288 @default.
- W2000632421 cites W2063606295 @default.
- W2000632421 cites W2064742164 @default.
- W2000632421 cites W2079379359 @default.
- W2000632421 cites W2083054665 @default.
- W2000632421 cites W2083262431 @default.
- W2000632421 cites W2083594431 @default.
- W2000632421 cites W2090149174 @default.
- W2000632421 cites W2104718805 @default.
- W2000632421 cites W2109337610 @default.
- W2000632421 cites W2155599995 @default.
- W2000632421 cites W2205090001 @default.
- W2000632421 doi "https://doi.org/10.1002/jssc.201200334" @default.
- W2000632421 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/22887899" @default.
- W2000632421 hasPublicationYear "2012" @default.
- W2000632421 type Work @default.
- W2000632421 sameAs 2000632421 @default.
- W2000632421 citedByCount "7" @default.
- W2000632421 countsByYear W20006324212013 @default.
- W2000632421 countsByYear W20006324212014 @default.
- W2000632421 countsByYear W20006324212015 @default.
- W2000632421 countsByYear W20006324212018 @default.
- W2000632421 countsByYear W20006324212019 @default.
- W2000632421 crossrefType "journal-article" @default.
- W2000632421 hasAuthorship W2000632421A5048729527 @default.
- W2000632421 hasAuthorship W2000632421A5051141279 @default.
- W2000632421 hasAuthorship W2000632421A5052534020 @default.
- W2000632421 hasAuthorship W2000632421A5065033176 @default.
- W2000632421 hasConcept C10390740 @default.
- W2000632421 hasConcept C119128265 @default.
- W2000632421 hasConcept C123460561 @default.
- W2000632421 hasConcept C161790260 @default.
- W2000632421 hasConcept C178790620 @default.
- W2000632421 hasConcept C179998833 @default.
- W2000632421 hasConcept C185592680 @default.
- W2000632421 hasConcept C2776923573 @default.
- W2000632421 hasConcept C2778576202 @default.
- W2000632421 hasConcept C2779854550 @default.
- W2000632421 hasConcept C40875361 @default.
- W2000632421 hasConcept C43617362 @default.
- W2000632421 hasConcept C4725764 @default.
- W2000632421 hasConceptScore W2000632421C10390740 @default.
- W2000632421 hasConceptScore W2000632421C119128265 @default.
- W2000632421 hasConceptScore W2000632421C123460561 @default.
- W2000632421 hasConceptScore W2000632421C161790260 @default.
- W2000632421 hasConceptScore W2000632421C178790620 @default.
- W2000632421 hasConceptScore W2000632421C179998833 @default.
- W2000632421 hasConceptScore W2000632421C185592680 @default.
- W2000632421 hasConceptScore W2000632421C2776923573 @default.
- W2000632421 hasConceptScore W2000632421C2778576202 @default.
- W2000632421 hasConceptScore W2000632421C2779854550 @default.
- W2000632421 hasConceptScore W2000632421C40875361 @default.
- W2000632421 hasConceptScore W2000632421C43617362 @default.
- W2000632421 hasConceptScore W2000632421C4725764 @default.
- W2000632421 hasLocation W20006324211 @default.
- W2000632421 hasLocation W20006324212 @default.
- W2000632421 hasOpenAccess W2000632421 @default.
- W2000632421 hasPrimaryLocation W20006324211 @default.
- W2000632421 hasRelatedWork W1724790200 @default.
- W2000632421 hasRelatedWork W1906032188 @default.
- W2000632421 hasRelatedWork W1974432954 @default.
- W2000632421 hasRelatedWork W1992312397 @default.
- W2000632421 hasRelatedWork W2060697271 @default.
- W2000632421 hasRelatedWork W2149258094 @default.