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- W2000633913 abstract "Two polyoxometallate-based compounds, tris[1,1′-(butane-1,4-diyl)bis(1 H -imidazol-3-ium)] bis[tetracosa-μ 2 -oxido-dodecaoxido-μ 12 -phosphato-dodecamolybdenum(VI)], (C 10 H 16 N 4 ) 3 [PMo 12 O 40 ] 2 , (I), and 1,1′-(butane-1,4-diyl)bis(1 H -imidazol-3-ium) 1-[4-(1 H -imidazol-1-yl)butyl]-1 H -imidazol-3-ium tetracosa-μ 2 -oxido-dodecaoxido-μ 12 -phosphato-dodecamolybdenum(VI) dihydrate, (C 10 H 16 N 4 )(C 10 H 15 N 4 )[PMo 12 O 40 ]·2H 2 O, (II), were synthesized by hydrothermal techniques at different pH values. The stoichiometric ratio between the polyoxometallate (POM) anions and organic cations is 2:3 in (I), with one of the cations lying on an inversion centre. The doubly protonated 1,1′-(butane-1,4-diyl)diimidazole (BIM) cations are linked to the [PMo 12 O 40 ] 3− anions by hydrogen bonds to form a three-dimensional supramolecular network. The stoichiometric ratio of POM anions and organic cations is 1:2 in (II), and the anion is located about a centre of inversion. The partly protonated BIM cations and solvent water molecules form hydrogen bonds with the [PMo 12 O 40 ] 3− anions, yielding a two-dimensional supramolecular layer. The different lattice architectures of (I) and (II) may be governed by the ratio between the POM anions and organic cations, which, in turn, is determined by the pH value." @default.
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- W2000633913 date "2013-05-10" @default.
- W2000633913 modified "2023-09-27" @default.
- W2000633913 title "Two polyoxometallate-based supramolecular compounds influenced by the ratio between the polyoxometallate anion and organic cation" @default.
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- W2000633913 doi "https://doi.org/10.1107/s0108270113011554" @default.
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