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- W2000638159 abstract "Abstract By using an arylthiolate ligand with a substituent in the para ‐position, 4‐ t BuC 6 H 4 S − , the yellow silver‐thiolate complex {[HNEt 3 ] 2 n [Ag 8 Ag 4/2 (SC 6 H 4 t Bu‐4) 12 ] n · n C 2 H 5 OH} ( 1 ) has been synthesized and structurally characterized. Complex 1 is ionic composed of [HNEt 3 ] + cations and a polymeric [Ag 8 Ag 4/2 (SC 6 H 4 t Bu‐4) 12 ] n 2 n − anion. Complex 1 reacts with CS 2 in acetone to give a red pentaconta‐nuclear silver anionic cluster complex {[HNEt 3 ] 4 [Ag 50 S 7 (SC 6 H 4 t Bu‐4) 40 ]·2CS 2 · 6C 3 H 6 O} ( 2 ). The core of the anionic cluster of 2 consists of fifty silver atoms and forty seven sulfur atoms, shaped like a discus with a diameter of ca. 2.0 nm. The factors influencing the structure and the formation mechanism of the large cluster are discussed. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)" @default.
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- W2000638159 date "2003-12-17" @default.
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- W2000638159 title "Synthesis and Crystal Structure of {[HNEt<sub>3</sub>]<sub>2<i>n</i></sub>[Ag<sub>8</sub>Ag<sub>4/2</sub>(SC<sub>6</sub>H<sub>4</sub><i>t</i>Bu‐4)<sub>12</sub>]<sub><i>n</i></sub>·<i>n</i>C<sub>2</sub>H<sub>5</sub>OH} and Its Reaction Product with CS<sub>2</sub>" @default.
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- W2000638159 doi "https://doi.org/10.1002/ejic.200300392" @default.
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