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- W2000644552 abstract "A cyclo dimetalated complex of Pt(II), [Bz2(C6H4CH2)P]2Pt, can be prepared from (η3-2-methylallylPtOAc)2 and PBz3. The X-ray structure determination of this complex is reported here. The crystals are triclinic(space group P1) with a = 16.536(2), b = 10.500(1) Å, α = 90.27(1), β = 95.16(3), γ = 83.84(2) deg, Z = 2, dc = 1.54 g cm−3. The structure was solved by Patterson and Fourier methods and refined by l.s. methods to a conventional R factor of 0.035, based on 4769 intensities above background. The molecule, of approximate C2 symmetry, shows a distorted square planar geometry, the metal atom being coordinated to two phosphorus atoms cis to each other and to two ortho carbon atoms of two phenyl rings again in mutual cis relation. The phosphines thus act as chelating ligands and the resulting five-membered PtCCC rings are puckered. The mean PtP and PtC distances are 2.277(2) and 2.067(7) Å respectively and the PPtP angle is 106.0(1)°." @default.
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- W2000644552 date "1980-01-01" @default.
- W2000644552 modified "2023-10-16" @default.
- W2000644552 title "The crystal and molecular structure of a Cis dimetalated complex of platinum(II)" @default.
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- W2000644552 doi "https://doi.org/10.1016/s0020-1693(00)92014-0" @default.
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