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- W2000647902 abstract "Abstract The effect of sodium 5‐sulfoisophthalic acid (NaSIPA) on the solid‐state polymerization of hexamethylenediammonium adipate was studied. In particular, different polyamide salt grades, such as a model salt of hexamethylenediamine and NaSIPA and a polyamide 6,6 salt containing NaSIPA, were prepared through alternative procedures based on the solution–precipitation technique. Furthermore, selected salt grades were solid‐state‐polymerized in a thermogravimetric analysis chamber under static and flowing nitrogen. Critical reaction parameters, such as the reaction temperature, surrounding gas, and presence of NaSIPA, were investigated to determine the rate‐controlling mechanism of the process. More specifically, NaSIPA significantly influenced solid‐state polyamidation by reducing the reaction rate and changing the prevailing mechanism. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 1609–1619, 2007" @default.
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- W2000647902 date "2007-02-26" @default.
- W2000647902 modified "2023-10-16" @default.
- W2000647902 title "Preparation and solid-state polyamidation of hexamethylenediammonium adipate: The effect of sodium 5-sulfoisophthalic acid" @default.
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- W2000647902 doi "https://doi.org/10.1002/app.25762" @default.
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